Personal Organic Synthesizer PPS-5511

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Personal Organic Synthesizer

• Adjustable test tube size, individual temperature control, and ramp function included

 

Model PPS-5511 

This is a personal organic synthesizer with five reaction vessels that enables a wide variety of liquid-phase application research to be performed quickly and efficiently. Individual temperature settings allow parallel synthesis experiments under different temperature conditions.

Equipped with a cooling water manifold, heating・cooling and stirring functions, the synthesis scale 0.5 to 60mL, and combination of different vessel sizes and types can be changed or added to accommodate condensation polymerization, sealed tube reactions, pressurized reactions, and etc.

 

♦ Accepts up to 5 reaction vessels

♦ Synthesis scale 0.5 to 60mL

♦ Temperature control -23℃ to 160℃ (5 individual controls) with accuracy ±0.5℃

♦ Rotation speed 10 to 2000rpm

♦ CE mark, RoHS compliance

 

PPS-5511 (reaction vessels, Dimroth condenser, pressure gauge, etc are sold separately)

 

◊ Powerful and efficient reflux experiments can be performed by connecting the cooling water manifold to the Dimroth condenser. The Dean-Stark trap can be used to remove water molecules during dehydration reactions.

◊ The cooling cartridge can be inserted from both the left and right sides.

◊ Sampling and titration with a dropping funnel are possible under inert conditions using a reaction vessel with branches or a three-way cock.

◊ Using sealed tubes, Schlenk flasks, pressure-resistant vessels, Dean-Stark traps, and others with gas sealing properties (vacuum to high pressure) and dehydration・deoxygenation functions, it is possible to create sealed tube, degassing・dehydrating・deoxygenating, high-pressure, and other atmospheres.

◊ It comes with a Teflon® shutter to prevent condensation on the aluminum block.

 

• Specifications

Product name Personal Organic Synthesizer : ChemiStation
Model PPS-5511
Cat. No. 226490
Stirrer Powerful magnetic stirrer
Reaction vessels・number of vessels Various reaction vessels・1 to 5 vessels (max. 20 pcs)
Synthesis scale 0.5 to 60mL (depends on reaction vessels)
Temperature control range -23 to 160℃ ( up to 130℃: 50 to 60mL), individual control  x 5 (cooling water circulator required)
Rotation speed range 100 to 2000rpm (1mL water: same rotation speed x 5), 100 to 1100rpm (60mL water: same rotation speed x 5)
Temperature setting・display Membrane keypad input・digital display (-40.0 to 160.0℃)
Temperature display resolution 0.1℃
Stirrer setting・display Speed control knob・digital display (20 to 2000rpm)
Reagent addition Pipette, syringe, dropping funnel (with taper joint) all allow reagent addition under inert condition
Gas displacement By vacuuming + introduction of inert gas (depends on vessel)
Reflux Optional reflux adapter/cooling water manifold
Observation window By slit in aluminum block (with illumination)
Safety features Earth leakage・overcurrent breaker, Thermal fuse, Temperature controller self-diagnostic function (variable upper temperature limit, sensor error), Double chamber, Drip receiving tray, Aluminum block loading detection, Motor overload protection
Temperature control・stirrer Includes PPS-CTRL1 model
Reaction vessels Diameter 13 to 35mm (max. insertion depth of 90 mm,supports more than 100 test tubes)
Wetted materials Glass, Teflon 
Cooling water port Cooling cartridge: hose 12mm OD, manifold: hose 12mm OD (cooling hose sold separately)
Gas port Reaction purge port: hose 9mm OD, Electric section air purge port: 6mm OD one-touch fitting
Taper joint NS14/23
Stirring bar Sold separately
Test tube adapter Sold separately
Reaction vessel related parts Sold separately
Manifold Includes PPS-55M1 model
Drip-proof cover Sold separately
Teflon® cap Sold separately
Aluminum block Includes PPS-55A1 model
Double chamber Includes PPS-55W1 model
Cooling cartridge Includes PPS-55LT1 model
Temperature control・stirrer Includes PPS-CTRL1 model
Ambient temperature range 5 to 35℃
Power input 6.5A, 650VA
Supply voltage 100VAC 50/60Hz
Outer dimensions (mm) 465W x 340D x 295H
Weight 23kg

◊ Performance values are based on 20°C, rated power supply voltage, no load, and use of cooling water circulator (Model NCB-2410).

◊ To perform temperature control below room temperature or reflux operations, connection to a cooling water circulator (CA-1117A/1330: -10°C) or NCB-2410 (refrigerant: ethanol -23°C) is required.

◊ Between adjacent blocks, the set temperature may be limited within certain conditions.

◊ For simultaneous gas substitution or reflux with cooling water circulation, the manifold (PPS-55M1) is convenient (up to 1hPa).

◊ Various reaction vessels, glass parts, test tube adapters, and reflux adapters are sold separately.

◊ Accessories

Manifold: Pole (1), Arbor (1), Pole holder (1), Silicone hose (diameter 5 x 8mm, 5m)
Temperature control・stirring section: CE conversion adapter (1), Fuse (2)

◊ A model without manifold is also available.

Product name Personal Organic Synthesizer : ChemiStation (without manifold)
Cat. No.  226500

 

• Components

Product name Manifold Aluminum block Double chamber Cooling cartridge Temperature control・Stirrer
Model PPS-55M1 PPS-55A1 PPS-55W1 PPS-55LT1 PPS-CTRL1
Cat. No. 226510 226390 226450 226420 226350

 

• Options

♦ Compatibility table for various adapters, condensers, drip-proof covers, and genuine reaction vessels

Test tube adapter Reflux adapter Drip-proof cover Cond- enser Reaction vessel
OD (mm) Number of tubes Reaction volume
(mL)
Availability 12 to
35mm OD
Availability Test tube Standard With branch Sealed With Teflon® cap With cock On-head pressure resistant vessel
12 1.2 Yes Yes No Yes
13 3 2 Yes Yes No
13 1 Yes Yes No
15 3 4 Yes Yes No Yes
15 1 Yes Yes No Yes Yes
16 1 4 Yes Yes No Yes
6 Yes Yes No
16.5 1 6 Yes Yes No
18 1 10  Yes Yes Yes Yes Yes Yes
20 1 10 Yes Yes
21 1 10 Yes Yes
24 1 10 Yes Yes Yes
24 1 12.5  Yes Yes Yes Yes Yes Yes Yes
25 1 14 No Yes
30※ 1 14 No Yes Yes
30 1 30 Yes Yes Yes Yes Yes
30 1 30 No Yes Yes Yes Yes Yes
34 1 60 No Yes Yes Yes Yes
35

(No adapter required)

60 No Yes Yes

※ Pressure-resistant vessel adapter 30mm OD

 

• A wide range of accessories for a diverse range of applications